Zn2SiO4 and SnO2 nanowires synthesized by thermal ramping technique

Authors: Zainal Abidin Ali, R. Puteh

Affiliations: Department of Physics, University of Malaya, 50603 Kuala Lumpur, Malaysia

Emails: zaba_87@yahoo.com; rustam@um.edu.my

Journal: International Journal of Fundamental Physical Sciences (IJFPS)

Volume: 1, Issue: 3, Pages: 64-67, Date: September, 2011

ISSN: 2231-8186

DOI: https://doi.org/10.14331/ijfps.2011.330016

Abstract

In this report, nanowires of Zn2SiO4 and SnO2 have been successfully synthesized using a simple novel method namely thermal ramping technique. The technique applies thermal ramping of the sample to a temperature of 900 °C using carbothermal reduction method. This technique requires no carrier gas. Elemental analysis and crystal structure were evaluated using Field Emission Scanning Electron Microscopy (FESEM), Energy Dispersive X-ray (EDX) and X-ray Diffraction (XRD) analysis. Nanowires of SnO2 and Zn2SiO4 with diameter ranging from 15–25 nm were observed. The effect of Au thickness in synthesizing Zn2SiO4 is also discussed.

Keywords

Thermal Ramping, Carbothermal Technique, SnO2 Nanowires

License: https://creativecommons.org/licenses/by/4.0/